Sodium Hydroxide → HCID 20200705, compound

HRID 979636Notes

Reaction equation

HRID 979636 reaction equation
C[O:2][C:3]([C:5]1[CH:24]=[CH:23][C:8]([CH2:9][N:10]([CH2:12][C:13]2[CH:18]=[CH:17][C:16]([C:19]([O:21]C)=[O:20])=[CH:15][CH:14]=2)[OH:11])=[CH:7][CH:6]=1)=[O:4].[OH-].[Na+]>>[C:3]([C:5]1[CH:6]=[CH:7][C:8]([CH2:9][N:10]([CH2:12][C:13]2[CH:18]=[CH:17][C:16]([C:19]([OH:21])=[O:20])=[CH:15][CH:14]=2)[OH:11])=[CH:23][CH:24]=1)([OH:4])=[O:2]

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 22222887HCID 22222887, compound

Product 1

HCID 20200705HCID 20200705, compound

Procedure

When N,N-bis(p-methoxycarbonylbenzyl)hydroxylamine, prepared in Example 1, is dissolved in an organic solvent and saponified with an aqueous sodium hydroxide solution, th above-named free acid compound is obtained after acidification with a mineral acid.

Workup

  1. dissolutionis dissolved in an organic solvent
  2. customis obtained after acidification with a mineral acid

Sources & evidence

ORD record
ord-66efd3eb04f04a5b8a29bfe4d9595091
Source dataset
uspto-grants-1987_05
Patent number
US04668727

Reaction notes

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