HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 979695Generated: October 27, 2026
Silane, ethenyltris(1-methylethoxy)- → 1,2-Bis(triisopropoxysilyl)ethylene
https://huagongshe.com/reaction/979695
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Silane, ethenyltris(1-methylethoxy)- | HCID 87409 | — |
| Reactant | Tris(propan-2-yloxy)silane | HCID 15722916 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 1,2-Bis(triisopropoxysilyl)ethylene | HCID 53828948 | — |
Reaction Steps
Into a 45 cc Parr bomb was added 2.5 g (0.012 mol) triisopropoxysilane, 5.7 g (0.024 mol) vinyltriisopropoxysilane, 1.0 xylene and 200 ppm Ru3CO12 (20 mg). The reaction was heated for 4 hours at 225° C. in a fluidized sand bath. A single product, 1,2-bis(triisopropoxysilyl)ethylene was formed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04668812 |
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| Source dataset | uspto-grants-1987_05 |
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| ORD ID | ord-1cfea45e05b949b0bff2e9a9f1f49b20 |
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| Source note | uspto-grants-1987_05 |
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