HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → Hydrogen Peroxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | N-(1-Oxodecyl)glycine | HCID 1712391 | — |
| Solvent | Methanesulfonic Acid | HCID 6395 | — |
| Product | Hydrogen Peroxide | HCID 784 | — |
| Product | N-(1-Oxodecyl)glycine | HCID 1712391 | — |
| Product | HCID 53638750 | HCID 53638750 | — |
Reaction Steps
N-Decanoylaminoperoxyacetic acid was prepared by reaction of N-decanoylglycine with hydrogen peroxide in methanesulfonic acid according to the procedure described in Example II. From 22.9 g (0.100 mol) of N-decanoylglycine and 17.0 g (0.500 mol) of hydrogen peroxide in 50 mL methanesulfonic acid was obtained 22.4 g of peroxyacid having an AvO of 6.06% (theoretical yield=24.5 g having an AvO of 6.53%), mp 75°-80° C. (melts with gas evolution).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04634551 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-154fd7f99743497f9376353c58da2260 |
| Source note | uspto-grants-1987_01 |