2-Amino-6-nitrobenzothiazole → HCID 73666081, compound

HRID 979789Notes

Reaction equation

HRID 979789 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:9][C:8]([CH2:10][S:11][CH2:12][CH2:13][NH:14][CH:15]=[C:16](SC)[N+:17]([O-:19])=[O:18])=[CH:7][CH:6]=1)[CH3:3].[NH2:22][C:23]1[S:24][C:25]2[CH:31]=[C:30]([N+:32]([O-:34])=[O:33])[CH:29]=[CH:28][C:26]=2[N:27]=1>>[CH3:3][N:2]([CH2:4][C:5]1[O:9][C:8]([CH2:10][S:11][CH2:12][CH2:13][NH:14][C:15]([NH:22][C:23]2[S:24][C:25]3[CH:31]=[C:30]([N+:32]([O-:34])=[O:33])[CH:29]=[CH:28][C:26]=3[N:27]=2)=[CH:16][N+:17]([O-:19])=[O:18])=[CH:7][CH:6]=1)[CH3:1]

Participants

3

Reactant 2

HCID 227042-Amino-6-nitrobenzothiazoleHCID 70430567HCID 70430567, compound

Product 1

HCID 73666081HCID 73666081, compoundYield 58%

Procedure

By reacting 1-[[[[5-(dimethylamino)methyl-2-furanyl]methyl]thio]ethylamino]-2-methylthio-2-nitroethene with 2-amino-6-nitrobenzothiazole, according to the procedure described in Example 4, the product was obtained in a 58% yield.

Workup

  1. customthe product was obtained in a 58% yield

Sources & evidence

ORD record
ord-6adbe41caa034fb8b0e013b1b30494c9
Source dataset
uspto-grants-1987_01
Patent number
US04634701

Reaction notes

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