HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 86741190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 8-Amino-6-methyl-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid | HCID 20222973 | — |
| Product | HCID 86741190 | HCID 86741190 | — |
Reaction Steps
The product from Example 140 was dissolved in methanol (50 ml) and concentrated sulfuric acid (3 ml) was added. The reaction was refluxed for 4 hours and solvent was evaporated to one-half the volume. Following the procedure of Example 136 the desired ester was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04634705 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-bc8bd6742c584b9d9950feda87a49a66 |
| Source note | uspto-grants-1987_01 |