Ethylenediamine → HCID 13753971, compound

HRID 979828Notes

Reaction equation

HRID 979828 reaction equation
[NH2:1][C:2]1[C:3]([Cl:14])=[C:4]2[C:9](=[CH:10][CH:11]=1)[CH:8]([C:12]#[N:13])[CH2:7][CH2:6][CH2:5]2.[CH2:15](N)[CH2:16][NH2:17]>>[ClH:14].[NH2:1][C:2]1[C:3]([Cl:14])=[C:4]2[C:9](=[CH:10][CH:11]=1)[CH:8]([C:12]1[NH:17][CH2:16][CH2:15][N:13]=1)[CH2:7][CH2:6][CH2:5]2

Participants

3

Reactant 2

HCID 3301EthylenediamineHCID 20222991HCID 20222991, compound

Product 1

HCID 13753971HCID 13753971, compoundYield 60%

Procedure

Utilizing the procedure of Example 74 with 6-amino-1-cyano-5-chloro-(1,2,3,4-tetrahydronaphthalene) (1.2 g) and ethylenediamine (3 ml) gave the desired compound in 60% yield. m.p. 220° C. (decomp.).

Sources & evidence

ORD record
ord-55038710ea3549b4a24f2e1175141756
Source dataset
uspto-grants-1987_01
Patent number
US04634705

Reaction notes

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