huagongshe.com
HRID979898

反应详情

EQUATION

反应方程式

HRID 979898 的结构方程式

REACTANTS

反应物

2
结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：CC(=O)Nc1ccc(N2CCNC2=O)cc1
HCID13755487

N-[4-(2-Oxoimidazolidin-1-yl)phenyl]acetamide

C11H13N3O2

PRODUCTS

生成物

1
结构：Nc1ccc(N2CCNC2=O)cc1
HCID13755491

1-(4-Aminophenyl)imidazolidin-2-one

C9H11N3O

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

A mixture of 10 g of 1-(p-acetamidophenyl)-2-imidazolidinone (see Example 1), 10 g of sodium hydroxide and 100 ml of water is heated under reflux for four hours. The product that crystallizes on cooling is collected and recrystallized from ethanol to yield 1-(4-aminophenyl)-2-imidazolidinone, m.p. 170°-2°.

WORKUP

后处理

  1. temperatureis heated
  2. temperatureunder reflux for four hours
  3. customThe product that crystallizes
  4. temperatureon cooling
  5. customis collected
  6. customrecrystallized from ethanol