Methyl iodide → HCID 19377717, compound

HRID 979924Notes

Reaction equation

HRID 979924 reaction equation
[CH3:1][O:2][CH:3]([O:10][CH3:11])[CH2:4][NH:5][C:6]([NH:8][CH3:9])=[S:7].[I:12][CH3:13]>CC(=O)C>[IH:12].[CH3:11][O:10][CH:3]([O:2][CH3:1])[CH2:4][NH:5][C:6]([S:7][CH3:13])=[N:8][CH3:9]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 14518105HCID 14518105, compound

Product 1

HCID 19377717HCID 19377717, compoundYield 99%

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of 7.1 parts of N-(2,2-dimethoxyethyl)-N'-methylthiourea, 8.5 parts of iodomethane and 80 parts of 2-propanone was stirred overnight. The reaction mixture was evaporated, yielding 12.8 parts (99%) of methyl N-(2,2-dimethoxyethyl)-N'-methylcarbamimidothioate monohydroiodide (191).

Workup

  1. customThe reaction mixture was evaporated

Sources & evidence

ORD record
ord-dd0e6e38489e45d6b7c35b911d8909ac
Source dataset
uspto-grants-1987_01
Patent number
US04634704

Reaction notes

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