HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2,3-dimethoxy-6-nitrobenzoate → Ethyl 2,3-dimethoxy-6-aminobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2,3-dimethoxy-6-nitrobenzoate | HCID 13749913 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 2,3-dimethoxy-6-aminobenzoate | HCID 13749914 | — |
Reaction Steps
Ethyl 2,3-dimethoxy-6-nitrobenzoate (200 g, 0.979 mole) was dissolved in ethanol (2 L) containing 5% palladium on carbon and hydrogenated until the theoretical amount of hydrogen was absorbed. Filtration and removal of the solvent in vacuo provided the product as a yellow oil, 220.6 g (98.0%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04634769 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-75ad21e1600f466aa715f7f6d9524b2b |
| Source note | uspto-grants-1987_01 |