HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Isoquinolinesulfonyl chloride → HCID 20159947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Isoquinolinesulfonyl chloride | HCID 3371655 | — |
| Reactant | HCID 20159907 | HCID 20159907 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 20159947 | HCID 20159947 | 83% |
Reaction Steps
The same procedure as described in Referential example 3 were repeated using 4.0 g of 5-isoquinolinesulfonyl chloride, 6.95 g of 4-t-butoxycarbonylamino-3-phenylbutylamine and 2.66 g of triethylamine, and there were obtained 6.6 g of N-(4-t-butoxycarbonylamino-3-phenylbutyl)-5-isoquinolinesulfonamide in a yield of 83%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04634770 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-4eb5b17794674a1682fc40e8ffd855d7 |
| Source note | uspto-grants-1987_01 |