HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxetane → 3-(4-Propyl-heptyl)-4-(3-hydroxypropyl)morpholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxetane | HCID 10423 | — |
| Reactant | 3-(4-Propylheptyl)morpholine | HCID 11096343 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-(4-Propyl-heptyl)-4-(3-hydroxypropyl)morpholine | HCID 19870277 | 86.2% |
Reaction Steps
A mixture of 22.7 grams (0.1 mole) of 3-(4-propyl-heptyl)morpholine, 6.4 grams (0.11 moles) trimethyleneoxide and 150 ml. 96% ethanol was kept at 150°-200° C. for 15 hours in an autoclave. Distillation of the reaction mixture gave 24.6 g (86%) of 3-(4-propyl-heptyl)-4-(3-hydroxypropyl)morpholine), boiling point 122°-124° C./0.01 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636382 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-fad4245dbc354722ba3c23de7711c6c4 |
| Source note | uspto-grants-1987_01 |