HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15657226, compound → HCID 276682, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15657226 | HCID 15657226 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 276682 | HCID 276682 | — |
Reaction Steps
10 g of compound (4) prepared above was suspended in 150 ml of acetone, and manganese dioxide was added thereto in an excess amount, followed by refluxing for 3 hours. Inorganic matter was removed by hot filtration, and the solvent was distilled off to obtain compound (5) as crystals. Yield: 4.5 g (45%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636456 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-de8eeb5a0f4e441ca9929962dbdd5c1a |
| Source note | uspto-grants-1987_01 |