Ammonia → HCID 13569202, compound

Participants

Reaction Steps

A mixture of ethyl 4-[2-(1-imidazolyl)ethoxy]phenoxyacetate free base (1.0 g), ethanol (10 ml) and concentrated ammonia solution (20 ml) was allowed to stand at room temperature for 20 hours to give a clear solution. The solution was evaporated and the residue was crystallised twice from 2-butanone to give 4-[2-(1-imidazolyl)ethoxy]phenoxyacetamide (0.38 g), m.p. 123°-124° C. Found: C, 59.70; H, 5.77; N, 16.26. C13H15N3O3 requires: C, 59.76; H, 5.79; N, 16.08%.

Provenance & Evidence