HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Disulfide → HCID 131715014, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | 2-Ethylaniline | HCID 11357 | — |
| Reactant | 2-Ethylphenyl isothiocyanate | HCID 2796213 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131715014 | HCID 131715014 | — |
Reaction Steps
A mixture of one molar proportion of 2-ethylaniline (EA) and 11.8 molar proportions of carbon disulfide in 4.3 molar proportions of ethanol was refluxed for about 16 hours, after which GC analysis showed that only a trace of the desired 2-ethylphenylisothiocyanate (EPI) had been formed to provide an EA/EPI area % ratio of 25/1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636574 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-823a5ed4b8a44985866773cc7030a4a9 |
| Source note | uspto-grants-1987_01 |