HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178472294, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 2-bromopropionate | HCID 79040 | — |
| Reactant | HCID 13107026 | HCID 13107026 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178472294 | HCID 178472294 | 39.7% |
Reaction Steps
By following the same procedure as in Example 10 using 1.8 g of 4-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-thioxo-4-imidazoline, 30 ml of dry acetone, 0.99 g of potassium carbonate, and 1.3 g of ethyl α-bromopropionate and recrystallizing the product from a mixture of toluene and cyclohexane, 0.95 g of ethyl 2-[4-(3,5-di-tert-butyl-4-hydroxyphenyl)-2-imidazolylthio]propionate was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636516 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-ae0783265f844418aca6df0b24fdd39f |
| Source note | uspto-grants-1987_01 |