HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium p-toluenesulfinate → 1H-Indole, 1-ethyl-2-methyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium p-toluenesulfinate | HCID 2723791 | — |
| Reactant | HCID 57213386 | HCID 57213386 | — |
| Product | 1H-Indole, 1-ethyl-2-methyl- | HCID 170432 | 86.1% |
Reaction Steps
Following a procedure similar to that described in Example 4A but employing 6.5 g. of 81.9% sodium p-toluenesulfinate, 6.3 g. of 95% 4-(benzylethylamino)benzaldehyde and 3.8 g. of 86.1% 1-ethyl-2-methyl-1H-indole, there was obtained 15.3 g. of 3-{[4-(benzylethylamino)phenyl](4-methylphenylsulfonyl)methyl}-1-ethyl-2-methyl-1H-indole as a gray tar-like product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636820 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-3db17ef830934a8e8fcf4725938ad711 |
| Source note | uspto-grants-1987_01 |