HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → Pyridinium, 1-dodecyl-, bromide (1:1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 1-Bromododecane | HCID 8919 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | Pyridinium, 1-dodecyl-, bromide (1:1) | HCID 66917 | — |
Reaction Steps
Equimolar amounts of 1-bromo-dodecane (249.2 g) and pyridine (79.1 g) are placed in a glass, three-necked, round bottom flask equipped with a heating means, a stirring means, and a condensing means. Then 82.1 g of isopropanol are added to the flask as a solvent. The contents of the vessel are heated to reflux with constant stirring. Reflux is maintained for six hours. Analysis of the reaction mixture indicates that the reaction is approximately 100 percent complete.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04637899 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-2faed7215f844b52838800e11d85d1f9 |
| Source note | uspto-grants-1987_01 |