2-Methylpyrazine → HCID 88655657, compound

HRID 980469Notes

Reaction equation

HRID 980469 reaction equation
[CH2:1]1[CH2:7][S:4](=[O:6])(=O)[O:3][CH2:2]1.[CH3:8][C:9]1[CH:14]=[N:13][CH:12]=[CH:11][N:10]=1>CCOCC.C(OCC)(=O)C>[S:4](=[CH:7][CH2:1][CH2:2][N:13]1[CH:12]=[CH:11][N:10]=[C:9]([CH3:8])[CH2:14]1)(=[O:6])=[O:3]

Participants

4

Reactant 2

HCID 79762-MethylpyrazineHCID 14264Propane sultone

Product 1

HCID 88655657HCID 88655657, compound

Reagents, catalysts & solvents 1

HCID 21584169Diethylether ethylacetateSolvent

Procedure

16.0 g of 1,3-propane sultone was dissolved in 200 ml of 1:1 ether/ethyl acetate and 15.1 g of 2-methylpyrazine added. It was then stored and the solvent allowed to evaporate.

Workup

  1. customto evaporate

Sources & evidence

ORD record
ord-e5768249d9f0460f8c4b92ad498b5222
Source dataset
uspto-grants-1987_01
Patent number
US04638005

Reaction notes

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