HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 13322003, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 13322002 | HCID 13322002 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 13322003 | HCID 13322003 | — |
Reaction Steps
To 10 g of (XXVIII) in 200 ml of ethyl acetate was added 5 ml of liquid ammonia with stirring at 0°. The mixture was allowed to attain room temperature, evaporated and the solid product was washed with ice-water. A dried sample of (XXV) had m.p. 242°-244°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04639265 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-d9eb10dd98d8435ebd8822463d4130bd |
| Source note | uspto-grants-1987_01 |