HuagongsheHuagongshe Chemistry Print Report · For research reference only
Caprolactam → 2-Isocyanatoethyl methacrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Caprolactam | HCID 7768 | — |
| Reactant | Di-n-butyldilauryltin | HCID 9809426 | — |
| Product | 2-Isocyanatoethyl methacrylate | HCID 35409 | — |
Reaction Steps
96.0 grams IEM was added to 77.0 grams (10% excess) caprolactam plus 0.17 grams dibutyltin dilaurate (DBTDL) under agitation at 75° C. over a period of 30 minutes, and held at 75° C. for a further 3 hours at which point the free NCO content had dropped to a trace by infrared spectroscopy. The product (IB) was a syrupy liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04639299 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-4f435d3d4ff44a159a761e452fdef6d5 |
| Source note | uspto-grants-1987_01 |