HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 13799024, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 131714665 | HCID 131714665 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13799024 | HCID 13799024 | — |
Reaction Steps
A solution of 5-methoxy-1-hydroxymethylbenzocyclobutene mesylate (38 g) and piperidine (45 ml) in toluene (180 ml) is refluxed under nitrogen for about 12 hours. The reaction mixture is filtered and the filtrate is evaporated in vacuo leaving a liquid residue which is used without further purification in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04639442 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-fc07bb8194284b638914880201e2ca1b |
| Source note | uspto-grants-1987_01 |