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Acetic Acid → Phenoxybutylamine acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Butyl isocyanide | HCID 76008 | — |
| 反応物 | 4-Phenoxybutan-1-amine | HCID 116240 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Phenoxybutylamine acetate | HCID 70062463 | — |
反応手順
In a three-necked flask of 25 ml provided with a magnetic bar, a calcium chloride tube and a dropping funnel, 1.99 gr (0.012 mol) of phenoxybutylamine, 1 gr (0.012 mol) of n-butylisonitrile and 0.72 gr of acetic acid were mixed in 5 ml of methanol. A precipitate of phenoxybutylamine acetate formed. This suspension cooled in an ice bath was added under good agitation with 0.87 gr (0.012 mol) of isobutyraldehyde.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04639468 |
| 出典データセット | uspto-grants-1987_01 |
| ORD ID | ord-6736ed9f75254637a52481ecc0d7be4d |
| 出典メモ | uspto-grants-1987_01 |