HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosuccinimide → Ethyl 5-chloro-2,3-dimethoxy-6-aminobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | Ethyl 2,3-dimethoxy-6-aminobenzoate | HCID 13749914 | — |
| Product | Ethyl 5-chloro-2,3-dimethoxy-6-aminobenzoate | HCID 13772052 | 55% |
Reaction Steps
Following the procedure employed in Example 27, treatment of ethyl 2,3-dimethoxy-6-aminobenzoate with N-chlorosuccinimide gave a 55% yield of the title compound after EtOH crystallization; mp 60-62%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04639518 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-0833daabc040409dae936f51cf4317e7 |
| Source note | uspto-grants-1987_01 |