HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 13361983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 3-Methoxybenzaldehyde | HCID 11569 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13361983 | HCID 13361983 | — |
Reaction Steps
A solution of 100 gm. of 3-methoxybenzaldehyde. 78.7 gm. of benzylamine, and 800 ml. of anhydrous ether was refluxed for 14 hours and then concentrated in vacuo to an oil. Distillation provided 144.3 gm. of clear oil, b.p. 152°-154° (1.2 Torr).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04639529 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-400aa91993c1450684c5ca483fd655cf |
| Source note | uspto-grants-1987_01 |