2,6-Lutidine → HCID 88660712, compound

Participants

Reaction Steps

Following the procedure of Preparation 2, but using p-nitrobenzyl 2-[3-(1-t-butyldimethylsilyloxyethyl)-4-methylthio-2-azetidinon-1-yl]-2-hydroxyacetate (470 mg), 2,6-lutidine (168 μl) and thionyl chloride (85 μl) and purifying the product by silica gel column chromatography eluted with methylene chloride, there were obtained 450 mg of the desired compound as an oil.

Provenance & Evidence