HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Disulfide → HCID 86741256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Hexamethyldisilazane | HCID 13838 | — |
| Reactant | Bromoacetyl bromide | HCID 61147 | — |
| Reactant | HCID 20220803 | HCID 20220803 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 86741256 | HCID 86741256 | — |
Reaction Steps
Following the procedure of Preparation 15, but using p-nitrobenzyl 2-(3-methoxy-4-methylthio-2-azetidinon-1-yl)-acetate (188 mg), hexamethyldisilazane (232 μl), butyllithium (0.68 ml), carbon disulphide (50 μl), and bromoacetyl bromide (48 μl), 108 mg of the desired product were obtained as an oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04639441 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-3b3ffe42b2e140eb94611dccab7ebe09 |
| Source note | uspto-grants-1987_01 |