HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → Benzene, 1,2-bis(phenylmethyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Diphenylmethane | HCID 7580 | — |
| Catalyst | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | Benzene, 1,2-bis(phenylmethyl)- | HCID 10934161 | 106.2% |
Reaction Steps
To a reaction vessel were added 2500 g of diphenylmethane and 40 g of aluminum chloride and reaction was carried out for 2 hours at room temperature with further adding 600 g of benzyl chloride with stirring. After the reaction, the catalyst was deactivated and 1300 g of a dibenzylbenzene isomer mixture (Composition I) was obtained by reduced pressure distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04639833 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-6e0c39a5328a430d8f3f2db1479452b7 |
| Source note | uspto-grants-1987_01 |