Dichloromethane → HCID 14235005, compound

HRID 981004Notes

Reaction equation

HRID 981004 reaction equation
[CH3:1][C:2]1([CH3:26])[C:23]2[C:6](=[CH:7][C:8]3[O:12][C:11]([C:13]4[CH:21]=[CH:20][C:16]([C:17](O)=[O:18])=[CH:15][CH:14]=4)=[N:10][C:9]=3[CH:22]=2)[C:5]([CH3:25])([CH3:24])[CH2:4][CH2:3]1.[Cl:27]CCl>>[CH3:1][C:2]1([CH3:26])[C:23]2[C:6](=[CH:7][C:8]3[O:12][C:11]([C:13]4[CH:21]=[CH:20][C:16]([C:17]([Cl:27])=[O:18])=[CH:15][CH:14]=4)=[N:10][C:9]=3[CH:22]=2)[C:5]([CH3:25])([CH3:24])[CH2:4][CH2:3]1

Participants

3

Reactant 2

HCID 6344DichloromethaneHCID 14234996HCID 14234996, compound

Product 1

HCID 14235005HCID 14235005, compound

Procedure

p-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphth[2,3-d]oxazolyl) benzoic acid (4.57 g - 13.1 mmoles) is suspended in dichloromethane (200 ml). There is then slowly added dicyclohexylamine (2.37 g - 13.1 mmoles) and the dichloromethane is then evaporated.

Workup

  1. customslowly added dicyclohexylamine (2.37 g - 13.1 mmoles) and the dichloromethane is then evaporated

Sources & evidence

ORD record
ord-86a3836394ba463ba32dcd755b908295
Source dataset
uspto-grants-1991_02
Patent number
USRE033533

Reaction notes

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