Diethyl Ether → HCID 53660533, compound

Participants

Reaction Steps

8.8 g of diatomaceous earth and a solution of 5.39 g of 12-pentyloxy-4,8-dodecadien-1-ol in 50 ml of dichloromethane were charged into a 250 ml flask. 8.8 g of PCC were then added in small portions and the mixture was stirred for 2 h at room temperature. Ethyl ether was added to the reaction mixture to precipitate the chromium salts, and the mixture was then filtered on SiO2, concentrated and distilled in a bulb-to-bulb apparatus. 4 g of 12-pentyloxy-4,8-cyclododecadien-1-one were obtained.

Provenance & Evidence