HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67830815, compound → HCID 11400846, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67830815 | HCID 67830815 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 11400846 | HCID 11400846 | — |
Reaction Steps
cis-N-(Benzyloxycarbonyl)azetidine-2,3-dicarboxylic acid, 10% Pd/C and methanol are hydrogenated under 3 atm of hydrogen in a Parr shaker for 4 hours. The catalyst is filtered off and thoroughly washed. The solution is evaporated to dryness and dried in vacuo to arrive at cis-azetidine-2,3-dicarboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04990504 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-80ed0bd2d48047ea9eb7f3198e11ba3f |
| Source note | uspto-grants-1991_02 |