HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 20071538, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 5-Chloroindole | HCID 87110 | — |
| Reactant | HCID 20071541 | HCID 20071541 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20071538 | HCID 20071538 | — |
Reaction Steps
A solution of 1.68 g 5-chloroindol (0.01 mole) and 1.50 g 2-nitroso-N-methyl-p-toluidine (0.01 mole), 10 ml acetic acid is boiled under reflux for 1 hour. Finally hydrogen bromide is introduced and the mixture is boiled for further 2 hours. After cooling it is poured into water. The dried reaction product is recrystallized from acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04990510 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-ed13e4fbd0e04456abf196e0fa07a951 |
| Source note | uspto-grants-1991_02 |