HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → N,N-diethyl-4-iodobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 4-Iodobenzoyl chloride | HCID 74373 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | N,N-diethyl-4-iodobenzamide | HCID 875218 | 89.7% |
Reaction Steps
4-Iodobenzoylchloride (10.0 g) was added portionwise to diethylamine (2.92 g) in triethylamine (40 ml) while the temperature was maintained at ca 20°. The resulting slurry was stirred at room temperature for 1 h, diluted with ER (150 ml), filtered and evaporated to give the title compound (10.2 g) m.p. 68°-70°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04990505 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-2fe8029bb8c142cda4f7fd156c625623 |
| Source note | uspto-grants-1991_02 |