HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20072181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 14149868 | HCID 14149868 | — |
| Product | HCID 20072181 | HCID 20072181 | — |
Reaction Steps
10.0 g of 2,4-dichloro-5-fluoro-3-iodo-benzoic acid and 9.5 ml of thionyl chloride are boiled until gas is no longer produced. The remaining thionyl chloride is then stripped off in vacuo. 10.2 g of crude acyl chloride, which can be employed without further purification, remain.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04990661 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-921df6fa5d084d01b9479de29eeb7404 |
| Source note | uspto-grants-1991_02 |