HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutylbenzene → 4'-Isobutylacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutylbenzene | HCID 10870 | — |
| Reactant | Acetyl fluoride | HCID 11204 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 4'-Isobutylacetophenone | HCID 93214 | — |
Reaction Steps
Isobutylbenzene (IBB) (10.2 lb/hr) and a solution of HF containing 13 wt % HOAc and 12 wt % acetyl fluoride (AcF) (153 lb/hr) were fed into reactor 1 through line 4. The mixture was reacted at 60° C. for 1.5 hrs to produce the desired 4-isobutylacetophenone product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04990681 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-d3b93062aae846dd972c13f70c9a7b8b |
| Source note | uspto-grants-1991_02 |