HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Diaminocyclohexane, trans- → HCID 54164031, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Diaminocyclohexane, trans- | HCID 43806 | — |
| Reactant | 1-Ethyl-6,7-difluoro-4-oxo-1,4-dihydroquinoline-3-carboxylic acid | HCID 800521 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 54164031 | HCID 54164031 | 66.3% |
Reaction Steps
A mixture of 2.53 g of 1-ethyl-6 7-difluoro-1,4- dihydro-4-oxo-3-quinolinecarboxylic acid and 4.6 g of trans-(-)-1,2-diaminocyclohexane in 10 ml of pyridine was reacted as described in Example 1 to give 2.3 g of the desired product, m.p. 230°-231°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04992449 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-f749f98412a045fea39add1d784b0936 |
| Source note | uspto-grants-1991_02 |