HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzaldehyde → HCID 20070365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzaldehyde | HCID 6996 | — |
| Reactant | 6-Amino-1,3-dimethyluracil | HCID 81152 | — |
| Reactant | Methyl 4-[2-(2,4,5-trimethylimidazol-1-yl)ethoxy]3-oxobutanoate | HCID 20070375 | — |
| Product | HCID 20070365 | HCID 20070365 | 4% |
Reaction Steps
The title compound (210 mg) was prepared from 2-chlorobenzaldehyde (1.4 g), 6-amino-1,3-dimethyl-2,4-dioxopyrimidine (1.55 g) and methyl 4-[2-(2,4,5-trimethylimidazol-1-yl)ethoxy]-3-oxobutanoate (2.68 g) by the method of Example 1. M.p. 226°-228° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04992447 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-49eaca29c46d446ca59fee64402b9f9d |
| Source note | uspto-grants-1991_02 |