HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzaldehyde → HCID 178498561, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzaldehyde | HCID 6996 | — |
| Reactant | Methyl 4-[2-(2,4,5-trimethylimidazol-1-yl)ethoxy]3-oxobutanoate | HCID 20070375 | — |
| Reactant | HCID 178507952 | HCID 178507952 | — |
| Product | HCID 178498561 | HCID 178498561 | 3% |
Reaction Steps
The title compound (110 mg) was prepared from 2-chlorobenzaldehyde (1.05 g), 2,4-diamino-6-hydroxypyrimidine (1.07 g) and methyl 4-[2-(2,4,5-trimethylimidazol-1-yl)ethoxy]-3-oxobutanoate (2.0 g) by the method of Example 1. M.p. 225°-227° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04992447 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-91bd0bf900344450b49d63a040290a98 |
| Source note | uspto-grants-1991_02 |