HCID 13956354, compound → HCID 53792600, compound

HRID 981592Notes

Reaction equation

HRID 981592 reaction equation
[CH3:1][O:2][C:3]1[C:8]([O:9][CH3:10])=[C:7]([O:11][CH3:12])[C:6]([CH3:13])=[CH:5][C:4]=1[OH:14].O[CH2:16][CH:17]=[C:18]([CH3:42])[CH2:19][CH2:20][CH:21]=[C:22]([CH3:41])[CH2:23][CH2:24][CH:25]=[C:26]([CH3:40])[CH2:27][CH2:28][CH:29]=[C:30]([CH3:39])[CH2:31][CH2:32][CH:33]=[C:34]([CH3:38])[C:35]([OH:37])=[O:36]>>[C:35]([C:34]([CH3:38])=[CH:33][CH2:32][CH2:31][C:30]([CH3:39])=[CH:29][CH2:28][CH2:27][C:26]([CH3:40])=[CH:25][CH2:24][CH2:23][C:22]([CH3:41])=[CH:21][CH2:20][CH2:19][C:18]([CH3:42])=[CH:17][CH2:16][C:5]1[C:4]([OH:14])=[C:3]([O:2][CH3:1])[C:8]([O:9][CH3:10])=[C:7]([O:11][CH3:12])[C:6]=1[CH3:13])([OH:37])=[O:36]

Participants

3

Reactant 2

HCID 13956354HCID 13956354, compoundHCID 54333183HCID 54333183, compound

Product 1

HCID 53792600HCID 53792600, compoundYield 59.8%

Procedure

The procedures of Example 1 were repeated except that 5 g of 2,3,4-trimethoxy-5-methylphenol and 3.2 g of 20-hydroxy-2,6,10,14,18-pentamethyl-2,6,10,14,18-eicosapentaenoic acid were employed as the starting materials to give 2.8 g of the title compound as a colorless oil.

Sources & evidence

ORD record
ord-03b2d62f876040ddaa368874111a61de
Source dataset
uspto-grants-1991_02
Patent number
US04992469

Reaction notes

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