HCID 13956354, compound → HCID 54340932, compound

HRID 981593Notes

Reaction equation

HRID 981593 reaction equation
[CH3:1][O:2][C:3]1[C:8]([O:9][CH3:10])=[C:7]([O:11][CH3:12])[C:6]([CH3:13])=[CH:5][C:4]=1[OH:14].O[CH2:16][CH:17]=[C:18]([CH3:47])[CH2:19][CH2:20][CH:21]=[C:22]([CH3:46])[CH2:23][CH2:24][CH:25]=[C:26]([CH3:45])[CH2:27][CH2:28][CH:29]=[C:30]([CH3:44])[CH2:31][CH2:32][CH:33]=[C:34]([CH3:43])[CH2:35][CH2:36][CH:37]=[C:38]([CH3:42])[C:39]([OH:41])=[O:40]>>[C:39]([C:38]([CH3:42])=[CH:37][CH2:36][CH2:35][C:34]([CH3:43])=[CH:33][CH2:32][CH2:31][C:30]([CH3:44])=[CH:29][CH2:28][CH2:27][C:26]([CH3:45])=[CH:25][CH2:24][CH2:23][C:22]([CH3:46])=[CH:21][CH2:20][CH2:19][C:18]([CH3:47])=[CH:17][CH2:16][C:5]1[C:4]([OH:14])=[C:3]([O:2][CH3:1])[C:8]([O:9][CH3:10])=[C:7]([O:11][CH3:12])[C:6]=1[CH3:13])([OH:41])=[O:40]

Participants

3

Reactant 2

HCID 13956354HCID 13956354, compoundHCID 53798267HCID 53798267, compound

Product 1

HCID 54340932HCID 54340932, compoundYield 51.2%

Procedure

The procedures of Example 1 were repeated except that 5 g of 2,3,4-trimethoxy-5-methylphenol and 3.5 g of 24-hydroxy-2,6,10,14,18,22-hexamethyl-2,6,10,14,18,22-tetracosahexaenoic acid were employed as the starting materials to give 2.5 g of the title compound as a colorless oil.

Sources & evidence

ORD record
ord-cc547746bfa140cdab134d2c099bd54e
Source dataset
uspto-grants-1991_02
Patent number
US04992469

Reaction notes

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