Aniline → HCID 54289289, compound

HRID 981721Notes

Reaction equation

HRID 981721 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:8]([C:11]12[CH2:17][CH:14]([CH:15]=[CH:16]1)[CH2:13][CH:12]2[C:18](Cl)=[O:19])[CH:9]=[CH2:10]>>[C:2]1([NH:1][C:18]([CH:12]2[CH2:13][CH:14]3[CH2:17][C:11]2([CH2:8][CH:9]=[CH2:10])[CH:16]=[CH:15]3)=[O:19])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 6115AnilineHCID 20070591HCID 20070591, compound

Product 1

HCID 54289289HCID 54289289, compound

Procedure

20.5 g of aniline and 39.3 g of allylbicyclo[2.2.1]hept-5-ene-2-carbonyl chloride are reacted in accordance with process A, affording 40.6 g (80.3% of theory) of a brown resin which is solid at room temperature and has a softening point of 66° C. The IR spectrum shows a band at 3300 cm-1 (--NH--) und at 1660 cm-1

Workup

  1. customaffording 40.6 g (80.3% of theory) of a brown resin which
  2. customat room temperature
  3. customa softening point of 66° C

Sources & evidence

ORD record
ord-7891a2c8103c4c759f484e5d60f7d4ac
Source dataset
uspto-grants-1991_02
Patent number
US04992518

Reaction notes

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