HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 14256487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 14256486 | HCID 14256486 | — |
| Catalyst | Benzoyl Peroxide | HCID 7187 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 14256487 | HCID 14256487 | 102.9% |
Reaction Steps
A mixture of 2,4-dimethoxy-6-methylquinazoline (8.2 g), N-bromosuccinimide (7.9 g), benzoyl peroxide (0.19 g) and carbon tetrachloride (200 ml) was heated to reflux for 2 hours. The warm solution was filtered and the filtrate was evaporated to give 6-bromomethyl-2,4-dimethoxyquinazoline (11.7 g), m.p. 138°-143° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04992550 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-b8fc0469323445a1a718e2b5674cdfdc |
| Source note | uspto-grants-1991_02 |