HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonate → 2-{[6-(4-Acetylphenyl)hexyl]oxy}-5-[3-(ethoxycarbonyl)benzoyl]benzenepropanoic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonate | HCID 85257 | — |
| Reactant | 5-[3-(Ethoxycarbonyl)benzoyl]-2-hydroxybenzenepropanoic acid ethyl ester | HCID 14739657 | — |
| Reactant | 6-(4-Acetylphenyl)hexanol | HCID 14739746 | — |
| Product | 2-{[6-(4-Acetylphenyl)hexyl]oxy}-5-[3-(ethoxycarbonyl)benzoyl]benzenepropanoic acid ethyl ester | HCID 14739790 | 80.3% |
Reaction Steps
In a manner analogous to Example 92B, 2.85 g of 6-(4-acetylphenyl)hexanol were converted into its mesylate and reacted with 1.78 g of 5-[3-(ethoxycarbonyl)benzoyl]-2-hydroxybenzenepropanoic acid ethyl ester to provide 2.21 g of the desired title product as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04992576 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-361ac484527745aa9e0a48bbed76f6e4 |
| Source note | uspto-grants-1991_02 |