Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Calcium Carbonate | HCID 10112 | — |
| Reactant | 2-Chloro-3-nitropyridine | HCID 79613 | — |
| Reactant | 2,4-Dimethylbenzene-1,3-diamine | HCID 4625581 | — |
| Product | HCID 20068349 | HCID 20068349 | — |
Reaction Steps
8.4 g of 2,4-diamino-m-xylene, 9.6 g of 2-chloro-3nitropyridine and 3.0 g of calcium carbonate were introduced into 300 ml water and the resulting mixture was heated under reflux for 8 hours to the boiling temperature. The reaction mixture was filtered while hot, the reaction product precipitating from the filtrate on cooling to 20° C. It was isolated and recrystallized from toluene. 6.2 g of the product melting at 173° to 175° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04994087 |
|---|
| Source dataset | uspto-grants-1991_02 |
|---|
| ORD ID | ord-83d842d100b547959c007af42c3def27 |
|---|
| Source note | uspto-grants-1991_02 |
|---|
