HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → 5-Nitro-2-[(2-phenylethyl)amino]benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 2-Fluoro-5-nitrobenzoic acid | HCID 280997 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | 5-Nitro-2-[(2-phenylethyl)amino]benzoic acid | HCID 2725582 | — |
Reaction Steps
A solution of 5.6 g of 2-fluoro-5-nitrobenzoic acid and 14.5 g of 2-phenylethylamine in 20 ml of dimethylacetamide is reacted and worked up in analogy to Example 1. Yellow crystals from isopropanol, melting point 116°-118° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04994493 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-d015d60566234c38ae731784bd91bdaa |
| Source note | uspto-grants-1991_02 |