HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 903133, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methyl Anthranilate | HCID 8635 | — |
| Reactant | Benzenepropanoyl chloride | HCID 64801 | — |
| Solvent | Methyl Acetate | HCID 6584 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 903133 | HCID 903133 | — |
Reaction Steps
A mixture of 17.6 g of 3-phenylpropanoyl chloride in 40 ml of ethyl acetate is added dropwise to a solution of 15.7 g of methyl anthranilate and 21 g of triethylamine in 60 ml of methyl acetate. The mixture is stirred at room temperature for 24 hours, water is added, and the organic phase is separated off and, after the solvent has been evaporated off, methyl 2-(3-phenylpropanoylamino)benzoate is obtained as an orange-colored oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04994493 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-a775b2fe06754d10bbcdbc5fb57fa602 |
| Source note | uspto-grants-1991_02 |