Acetyl chloride → 2-(4-Isobutylphenyl)acrylonitrile

HRID 982180Notes

Reaction equation

HRID 982180 reaction equation
[CH2:1]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)[CH:2]([CH3:4])[CH3:3].[C-:11]#[N:12].[Na+].[C:14](Cl)(=O)[CH3:15].[Cl-].[Al+3].[Cl-].[Cl-]>>[C:11]([C:14]([C:8]1[CH:9]=[CH:10][C:5]([CH2:1][CH:2]([CH3:4])[CH3:3])=[CH:6][CH:7]=1)=[CH2:15])#[N:12]

Participants

5

Reactant 4

HCID 6367Acetyl chlorideHCID 8929Sodium CyanideHCID 10870IsobutylbenzeneHCID 6451240Aluminum(III) Chloride

Product 1

HCID 132277082-(4-Isobutylphenyl)acrylonitrile

Procedure

A process which comprises reacting isobutylbenzene with sodium cyanide and acetyl chloride in the presence of aluminum chloride at a temperature of about 60°-120° C. to form 1-cyano-1-(4-isobutylphenyl)ethene.

Workup

  1. customat a temperature of about 60°-120° C.

Sources & evidence

ORD record
ord-19fb70b8007c4168b87356811d515bd5
Source dataset
uspto-grants-1991_02
Patent number
US04994596

Reaction notes

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