HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonamide, 4-methyl-N-phenyl- → N-[4-[(1-acetyl-4-piperidinyl)carbonyl]phenyl]Methanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonamide, 4-methyl-N-phenyl- | HCID 2456 | — |
| Reactant | 1-Acetylpiperidine-4-carbonyl chloride | HCID 100950 | — |
| Reactant | N-benzoylnipecotoyl chloride | HCID 15718173 | — |
| Product | N-[4-[(1-acetyl-4-piperidinyl)carbonyl]phenyl]Methanesulfonamide | HCID 14130038 | — |
Reaction Steps
The same procedure as above was repeated except that methanesulfonamilide was replaced with p-toluenesulfonanilide or 1-acetylisonipecotoyl chloride was replaced with (±)-N-benzoylnipecotoyl chloride or (±)-N-benzoyl-β-prolyl chloride prepared in Referential Example 2 to obtain the following compounds:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04996215 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-988a5fe0588949808d1ed8199a9ee096 |
| Source note | uspto-grants-1991_02 |