Dibenzyl ether → HCID 20067720, compound

HRID 982430Notes

Reaction equation

HRID 982430 reaction equation
[C:1]1([C:7]([CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:16]([O:23][CH2:24][C:25]1C=CC=CC=1)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1.BrC(O)C>>[CH2:16]([O:23][CH2:24][CH2:25][CH:9]([C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1)[C:7]([C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)=[O:8])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

Participants

4

Reactant 3

HCID 7657Dibenzyl etherHCID 99482-PhenylacetophenoneHCID 14202443Ethanol, 1-bromo-

Product 1

HCID 20067720HCID 20067720, compound

Procedure

This compound is prepared from 19.6 g of desoxybenzoin and 21.5 g of benzylether-protected bromoethanol according to the procedure described in Example 1(a).

Sources & evidence

ORD record
ord-7148a9d4a91e4902b81446e47d06d3ec
Source dataset
uspto-grants-1991_02
Patent number
US04996225

Reaction notes

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