2-Phenylacetophenone → HCID 20067684, compound

HRID 982435Notes

Reaction equation

HRID 982435 reaction equation
[C:1]1([C:7]([CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[O:16]1[CH2:21][CH2:20][CH2:19][CH2:18][CH:17]1[O:22][CH:23]1[CH2:28][CH2:27]CCO1.BrCCCO>>[O:16]1[CH2:21][CH2:20][CH2:19][CH2:18][CH:17]1[O:22][CH2:23][CH2:28][CH2:27][CH:9]([C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1)[C:7]([C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)=[O:8]

Participants

4

Reactant 3

HCID 99482-PhenylacetophenoneHCID 123083-Bromo-1-propanolHCID 263182Tetrahydropyranyl ether

Product 1

HCID 20067684HCID 20067684, compound

Procedure

The compound is prepared from 19.6 g of desoxybenzoin and 22.3 g of tetrahydropyran-2-yl ether-protected 3-bromopropanol according to the procedure described in Example 1(a).

Sources & evidence

ORD record
ord-92fca0584e90410e91701696d1e8efbf
Source dataset
uspto-grants-1991_02
Patent number
US04996225

Reaction notes

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