HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenylacetophenone → HCID 20067692, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenylacetophenone | HCID 9948 | — |
| Reactant | Ethane, 2-bromo-1,1-diethoxy- | HCID 74852 | — |
| Catalyst | Benzyl triethylammonium chloride | HCID 66133 | — |
| Catalyst | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| Product | HCID 20067692 | HCID 20067692 | — |
Reaction Steps
The compound is prepared from 19.6 g of desoxybenzoin and 19.7 g of bromacetaldehyde diethyl acetal according to the procedure in Example 1(a). The reaction is performed however at 90° C. and using TBAH as catalyst instead of TEBAC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04996225 |
| Source dataset | uspto-grants-1991_02 |
| ORD ID | ord-4f34f6e1ac5a43fea058ea72d3eae543 |
| Source note | uspto-grants-1991_02 |